"Interrupted Barton-Zard/Friedel-Crafts Alkylation Telescoped Reaction for the Synthesis of Pyrrolo[3,4-b]indole Cores Bearing Multiple Aryl Substituents"
Dataset: nmr.zip, 64.66 MB Access Condition: Embargo period 2025-02-27 Description: Raw 1H and 13C NMR data for compounds 1m-o, 2c-m, 3-27, raw 2D NMR spectra for compound 3. Spectra can be opened with commercially available programs MestReNova and TopSpin, or SpinWorks (freeware). File that needs to be opened is located in "Compound name"\1H (or 13C)\pdata\1\procs. (English)
Dataset: ftir.zip, 4.46 MB Access Condition: Embargo period 2025-02-27 Description: Data as generated by the instrument's software PerkinElmer Spectrum IR Version 10.6.1. Data can be opened with any .pdf reader. (English)
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Cite this document
Gredičak, M. (2025). "Interrupted Barton-Zard/Friedel-Crafts Alkylation Telescoped Reaction for the Synthesis of Pyrrolo[3,4-b]indole Cores Bearing Multiple Aryl Substituents" [Data set]. https://urn.nsk.hr/urn:nbn:hr:241:450511.
Gredičak, Matija. "Interrupted Barton-Zard/Friedel-Crafts Alkylation Telescoped Reaction for the Synthesis of Pyrrolo[3,4-b]indole Cores Bearing Multiple Aryl Substituents". Institut Ruđer Bošković, 2025. 28 Feb 2025. https://urn.nsk.hr/urn:nbn:hr:241:450511.
Gredičak, Matija. 2025. "Interrupted Barton-Zard/Friedel-Crafts Alkylation Telescoped Reaction for the Synthesis of Pyrrolo[3,4-b]indole Cores Bearing Multiple Aryl Substituents". Institut Ruđer Bošković. https://urn.nsk.hr/urn:nbn:hr:241:450511.
Gredičak, M. 2025. "Interrupted Barton-Zard/Friedel-Crafts Alkylation Telescoped Reaction for the Synthesis of Pyrrolo[3,4-b]indole Cores Bearing Multiple Aryl Substituents". Institut Ruđer Bošković. [Online]. [Accessed 28 February 2025]. Available from: https://urn.nsk.hr/urn:nbn:hr:241:450511.
Gredičak M. "Interrupted Barton-Zard/Friedel-Crafts Alkylation Telescoped Reaction for the Synthesis of Pyrrolo[3,4-b]indole Cores Bearing Multiple Aryl Substituents". [Internet]. Institut Ruđer Bošković; 2025, [cited 2025 February 28] Available from: https://urn.nsk.hr/urn:nbn:hr:241:450511.
M. Gredičak, "Interrupted Barton-Zard/Friedel-Crafts Alkylation Telescoped Reaction for the Synthesis of Pyrrolo[3,4-b]indole Cores Bearing Multiple Aryl Substituents", Institut Ruđer Bošković, 2025. Accessed on: Feb 28, 2025. Available: https://urn.nsk.hr/urn:nbn:hr:241:450511.
"Interrupted Barton-Zard/Friedel-Crafts Alkylation Telescoped Reaction for the Synthesis of Pyrrolo[3,4-b]indole Cores Bearing Multiple Aryl Substituents"
Scientific / art field, discipline and subdiscipline
NATURAL SCIENCES Chemistry Organic Chemistry
Abstract (english)
Experimental set includes raw 1H and 13C NMR data for compounds 1m-o, 2c-m, 3-27, raw 2D NMR spectra for compound 3, and FTIR .pdf reports as generated by the IR instrument from which signals were assigned.
Data is for the reviewing process. Data will be changed (renamed, added, removed) as per the result of the reviewing process, to be in line with the accepted paper.
Methods (english)
NMR spectra were recorded on Bruker Avance 600 and 300 MHz spectrometers, operating at 150.92 or 75.47 MHz for 13C and 600.13 or 300.13 MHz for 1H nuclei. Chemical shifts are quoted in ppm and are referenced to the residual nondeuterated solvent peak. Spectra were acquired at 298 K.
Infrared spectra were recorded on a Varian UV/Vis Cary 4000 spectrometer equipped with an attenuated total reflectance attachment with internal calibration.
Number: IP-2022-10-5184 Title (croatian): Organokatalitičke dearomatizacijske strategije inspirirane prirodnim spojevima Acronym: OCADA Leader: Matija Gredičak Jurisdiction: Croatia Funding stream: Research Projects
Publisher
Institut Ruđer Bošković Ruđer Bošković Institute
Access conditions
Open access
Terms of use
Public note (english)
Data is for the reviewing process. Data will be changed (renamed, added, removed) as per the result of the reviewing process, to be in line with the accepted paper.